General Description
The modern material science uses a wide range of measuring techniques and competences.
Between the families of interesting materials for the new century, ceramics and high temperature materials play key roles for extremely demanding fields.
For a deep knowledge of them, the researcher must rely on high performance instruments, easy to use and with a high degree of reliability.
AMEL, thanks to a long timed experience and a continuous development program in close contact with leading laboratories, has developed the first integrated system for high temperature electrochemical experiment: 698 oven and cell. Have a closer view of the connection to the cell.
This unit allows you to run both classical electrochemical experiments or EIS scanning up to 1200 C°, with complete control of the environment around the sample. Have a close view of the front control panel.
2, 3 or 4 wires connections are available, and an integral guarding system that let you reach high impedances without the artefacts usually related to the sample holder.
A family of optional devices will help the researcher to fit specific needs in a flawlessly integration.
Let focus on the real problems and allow AMEL to solve your high temperature problems!
Technical Specifications
| OVEN |
| Temperature range |
0-1200 C° |
| Controller |
Eurotherm 2216e |
| Thermocouple |
Type S |
| Interface |
RS-232 serial port |
| Communication protocol |
MODBUS |
| Orientation |
Vertical |
| Loading |
From the bottom |
| Controlled atmosphere |
Gas and primary vacuum allowed |
| Other features |
- Electric lift for the sample holder
- Gas in pressure reducer
- Gas out valve
- Inner pressure dial readout
|
| SAMPLE HOLDER |
| Sample dimension |
15 mm max diameter 6 mm thickness |
| Connections |
2-wire standard connection |
|
wire compensation or true 4-wire connections optional |
| Signal connections |
BNC |
| Guarding /shielding |
Integral on the red contacts, sensing electrode included in the shield |
| Maximum current |
Up to 1 A depending on the working temperature |
| Insulating material |
Allumina 99.5 % rods Allumina bisquit 99.5 % plates |
| Contacts |
Platinum 99.5% 0.3 mm thickness 10 mm dia plates |
|
Different shapes depending on options and request |
| Contact placing |
Spring loaded plates (variable sample pressure optional) |
| Contact resistance |
1.5 Ohm (2-wire 25 C°) |
|
0.005 Ohm residual (two wire with compensation or 4-wire connection) |
| Sample temperature monitoring |
Allumina well that reaches the top plate of the holder |
| OPTIONS |
| Connections |
4-WIRE or compensated wire connections |
| Pressure |
Variable pressure of the sample up to 5 N |
| Thickness measurement |
Coaxial micrometer for thermal expansion measure, relative measurements only 1um max resolution, RS-232 connection and Termoplot software |
| Sticky and melting samples |
Contact the factory for possible options and details |
| Sample temperature |
Second controller with readout, RS-232 interface and Termoplot software (including cables and thermocouple) |
| POWER SUPPLY AND SIZE |
| Voltage mains |
115 / 230 V ranges (+/- 10%) |
| Power consumption |
1500 VA max |
| Size & weight |
Approx 450 x 430 x 630 mm (L x W x H) Kg 12 |